Journals / Cumhuriyet Science Journal / 2018 / Cilt: 39 - Sayı: 33

Optimization Of Extraction Parameters For Folic Acid And Antioxidant Compounds From An Edible Plant (Polygonum Cognatum Meissn) Using Pressurized Liquid Extraction (PLE) System

Yenilebilir Bir Bitki Olan Polygonum Cognatum Meissn dan Folik Asit ve Antioksidan Bileşiklerin Basınçlı Sıvı Ekstraksiyon (PLE) sistemi ile Ekstraksiyonu için Optimal Koşulların Belirlenmesi

Pages
1069–1080
Publication Date
2022-10-12
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Although antioxidant activity levels differ depending on solvent components, the similar results were obtained such in the other optimization parameters.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:Madimak (Polygonum cognatum Meissn.) plant is a wild edible plant with a cosmopolitan distribution and also traditionally consumed as food in anatolia.
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Key Findings & Data:A solvent including 1 M NaOH and water (1:99), 60 min of extraction time, 40 oC of extraction temperature and 1500 psi of pressure were optimized and found as the most productive operating conditions for PLE in the folic acid determination.
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Conclusion & Impact:Although antioxidant activity levels differ depending on solvent components, the similar results were obtained such in the other optimization parameters.
🔬Design:Modeling & Simulation
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

Madimak (Polygonum cognatum Meissn.) plant is a wild edible plant with a cosmopolitan distribution and also traditionally consumed as food in anatolia. This study aims to optimize the extraction parameters in the pressurized liquid extraction (PLE) system and to search some beneficial properties of this plant. After the optimal extraction conditions was determined, the effect of PLE conditions on antioxidant properties was studied by using plant extracts in terms of total phenolic contents, free radical scavenging capacities and reducing power. A solvent including 1 M NaOH and water (1:99), 60 min of extraction time, 40 oC of extraction temperature and 1500 psi of pressure were optimized and found as the most productive operating conditions for PLE in the folic acid determination. Mainly, optimization of PLE conditions were carried out by considering folic acid amounts. Although antioxidant activity levels differ depending on solvent components, the similar results were obtained such in the other optimization parameters.

Özet

Madımak (Polygonum cognatum Meissn) bitkisi geleneksel olarak Anadolu’da gıda olarak tüketilen, kozmopolitan bir dağılıma sahip kendiliğinden yetişenbir bitkidir. Bu çalışma temelde bu bitkinin yararlı özelliklerini ortaya çıkarmak adına basınçlı sıvı ekstraksiyon sisteminin optimizasyonunu amaçlar. Optimal koşullar belirlendikten sonra, ekstraksiyon koşullarının antioksidan özellikler üzerine etkisi, toplam fenolik içerik, serbest radikal süpürücü etki ve indirgeme gücü özelinde değerlendirildi. İdeal optimizasyon koşullarının 1 M NaOH ve suyun (1:99) çözegen karışımı ile, 60 dk boyunca , 40 oC sıcalıkta, 1500 psi basınçta folik asit için en ideal olduğu belirlendi. Temelde, antioksidan aktivite için gerekli koşullar folik asit için yapılan optmizasyonlar dikkate alınarak belirlenmiştir. Elde edilen sonuçlara göre antioksidan aktivite seviyelerinin çözücü bileşiminden etkilendiği aynı şekilde diğer optimizasyon parametrelerin de değişkenlik gösterdiği gözlenmiştir.

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Cite This Article

ATEŞ, B., ERDOĞAN, S., ERDEMOĞLU, S., ULUSOY, H. İ., ULUSOY, S., KARASLAN, M. G. (2022). Optimization Of Extraction Parameters For Folic Acid And Antioxidant Compounds From An Edible Plant (Polygonum Cognatum Meissn) Using Pressurized Liquid Extraction (PLE) System. Cumhuriyet Science Journal, Cilt: 39 - Sayı: 33, 1069–1080. https://ajindex.com/articles/477908

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References (11)

  1. Ulusoy S., Acidereli H., Erdogan S., Ulusoy H.I., A new approach to the determination of folic acid at trace levels: using a Fe(III)-folic acid complex to amplify analytical signal, RSC Adv., 6 (2016) 40115-40122.
  2. Biesalski H.K., Tinz J. Multivitamin/mineral supplements: Rationale and safety, Nutrition, 33 (2017) 60-66.
  3. Gregory J.F., Quinlivan E.P., Davis S.R,. Integrating the issues of folate bioavailability, intake and metabolism in the era of fortification. In: Trends in Food Science and Technology., Trends Food Sci Technol., 16 (2005) 229-240.
  4. Ulusoy H.I., Acıdereli H., Ulusoy S., Erdogan S., Development of a New Methodology for Determination of Vitamin B9 at Trace Levels by Ultrasonic-Assisted Cloud Point Extraction Prior to HPLC, Food Anal. Methods, 10 (2017) 799-808.
  5. Uusiku N.P., Oelofse A., Duodu K.K.G, Bester M.J., Faber M., Nutritional value of leafy vegetables of sub-Saharan Africa and their potential contribution to human health: A review, Journal of Food Composition and Analysis, 23 (2010) 499-509.
  6. Rahimi R., Goodarzi N., Determination of Folic Acid in Mint Vegetable, by High-Performance Liquid Chromatography, Org.Chem., 1 (2011) 31-35.
  7. Thomas P.M., Flanagan V.P., Pawlosky R.J., Determination of 5-methyltetrahydrofolic acid and folic acid in citrus juices using stable isotope dilution - Mass spectrometry, J. Agric. Food Chem., 51 (2003) 1293-1296.
  8. Iyer R., Tomar S.K,. Determination of folate/folic acid level in milk by microbiological assay, immuno assay and high performance liquid chromatography, J. Dairy Res., 80 (2013) 233. Ringling C., Rychlik M., Analysis of seven folates in food by LC-MS/MS to improve accuracy of total folate data, Eur. Food Res. Technol., 236 (2013) 17-28.
  9. Verwei M., Arkbage K., Havenaar R., van den Berg H., Witthoft C., Schaafsma G., Folic acid and 5-methyltetrahydrofolate in fortified milk are bioaccessible as determined in a dynamic in vitro gastrointestinal model, J Nutr., 133 (2003) 2377-2383.
  10. Alonso-Salces R.M., Korta E., Barranco A., Berrueta L.A., Gallo B., Vicente F., Determination of polyphenolic profiles of Basque cider apple varieties using accelerated solvent extraction, J. Agric. Food Chem., 49 (2001) 3761-3767. Zafra-Gómez A., Garballo A., Morales J.C., García-Ayuso L.E., Simultaneous determination of eight water-soluble vitamins in supplemented foods by liquid chromatography, J. Agric. Food Chem., 54 (2006) 4531-4536.
  11. Ulusoy H.I., Acıdereli H., Tutar U., Optimization of Extraction Parameters for Fat-Sol