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Journals / Sigma Mühendislik ve Fen Bilimleri Dergisi / 2020 / Cilt: 38 - Sayı: 1

Synthesis, characterization and thermal properties of new oxoethyl acrylate containing polymer

Nevin ÇANKAYA
Pages
281–288
Publication Date
2020-03-27
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Homopolymer synthesized is also characterized by spectroscopic techniques and thermal characterization is investigated by TGA/DTA/DTG thermal analysis methods.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:In this study, 2-(bis(cyanomethyl)amino)-2-oxoethyl acrylate (CMA2OEA) monomer, which does not exist in the literature, was synthesized and characterized.
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Key Findings & Data:Elemental analysis technique, along with classical spectroscopic methods such as FTIR, 1H and 13C NMR, is used in the characterization of the monomer.
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Conclusion & Impact:Homopolymer synthesized is also characterized by spectroscopic techniques and thermal characterization is investigated by TGA/DTA/DTG thermal analysis methods.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:2-(bis(cyanomethyl)amino)-2-oxoethyl acrylate (CMA2OEA) · poly(CMA2OEA) · monomer

Abstract

In this study, 2-(bis(cyanomethyl)amino)-2-oxoethyl acrylate (CMA2OEA) monomer, which does not exist in the literature, was synthesized and characterized. Elemental analysis technique, along with classical spectroscopic methods such as FTIR, 1H and 13C NMR, is used in the characterization of the monomer. Further, homopolymer of the CMA2OEA monomer [poly(CMA2OEA)] is synthesized by free radical chain polymerization reaction. Homopolymer synthesized is also characterized by spectroscopic techniques and thermal characterization is investigated by TGA/DTA/DTG thermal analysis methods.

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Cite This Article

ÇANKAYA, N. (2020). Synthesis, characterization and thermal properties of new oxoethyl acrylate containing polymer. Sigma Mühendislik ve Fen Bilimleri Dergisi, Cilt: 38 - Sayı: 1, 281–288. https://ajindex.com/articles/419303

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References (9)

  1. Barım G., Coşkun M. (2012) (2,3-Difenil-1,3-oksazolidin-5-il)metil metakrilat’ın metil metakrilat ile kopolimerlerinin sentezi, karakterizasyonu ve termal özellikleri. Adıyaman Üniversitesi Fen Bilimleri Dergisi. 2 (2), 75-85
  2. Zengin H.B., Basan S., Ekberov O.H. (2005) Maleik Anhidrit–Stiren Kopolimerinin Amid ve İmid Türevlerinin Sentezi ve Isısal Davranışları. Cumhuriyet Üniversitesi Fen Bilimleri Dergisi. 26 (2), 1-21
  3. Soykan C., Yakuphanoglu, F., Sahin, M. (2013) Synthesis, Antimicrobial Activity and Semi-conducting Properties of Novel 2-(4-Chloro-1-Naphtyloxy)-2-Oxoethyl Methacrylate with 2-(Diethylamino)Ethyl Methacrylate Copolymers. Journal of Macromolecular Science, Part A: Pure and Applied Chemistry. 50, 953–965 [4] Hemalatha P., Veeraiah M. K., Prasanna Kumar S., Madegowda N. M., Manju M. (2014) Reactivity Ratios of N-Vinylpyrrolidone-Acrylic Acid Copolymer. American Journal of Polymer Science. 4 (1), 16-23
  4. Çankaya N., Besci G. (2018) Synthesis, characterization, thermal properties and reactivity ratios of methacrylate copolymers including methoxy group, Journal of the Faculty of Engineering and Architecture of Gazi University. 33 (3), 1155-1170
  5. Rajdeo K.S., Ponrathnam S., Pardeshi S., Chavan N.N., Bhongale S.S, Harikrishna R. (2015) Ambient Temperature Photocopolymerization of Tetrahydrofurfuryl Methacrylate and Isobornyl Methacrylate: Reactivity Ratios and Thermal Studies. Journal of Macromolecular Science, Part A: Pure and Applied Chemistry. 52, 982-991
  6. Bayram O. (2019) Wettability, optical and chemical characteristics of plasma-polymerized D-limonene thin films. Omer Halis University Journal of Enginering Sciences. 8 (1), 567-575
  7. Ilter Z., Soykan C., Solmaz A. (2015) Copolymers of 7-Methoxy-2-Acetyl Benzofuryl Methylmethacrylate with Styrene: Synthesis, Characterization, Reactivity Ratios and Determination of Kinetic Parameters with Thermogravimetric Analysis. Journal of Macromolecular Science, Part A: Pure and Applied Chemistry. 52, 175–185
  8. Patel J. N., Dolia M. B., Patel K. H., Patel R. M. (2006) Homopolymer of 4-chloro-3-methyl Phenyl Methacrylate and its Copolymers with Butyl Methacrylate: Synthesis, Characterization, Reactivity Ratios and Antimicrobial Activity. Journal of Polymer Research. 13, 219-228
  9. Açıkbaş Y., Çankaya N., Capan R., Erdogan M., Soykan C. (2016) Swelling behavior of the 2-(4-methoxyphenylamino)-2-oxoethyl methacrylate monomer LB thin film exposed to various organic vapors by q