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Journals / Sigma Mühendislik ve Fen Bilimleri Dergisi / 2016 / Cilt: 34 - Sayı: 2

SYNTHESIS AND THERMAL PROPERTIES OF NOVEL MALEONITRILES

Ali ERDOĞMUŞ
Pages
153–158
Publication Date
2016-06-01
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Both compounds are characterized by IR, Mass, NMR spectroscopy as well as elemental analysis.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:In this study, the synthesis and thermal properties of two novel maleonitriles bearing 8-membered heterocyclic derivatives is described first time.
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Key Findings & Data:New maleonitriles, benzo-(1,2-bis-methylthio)maleonitrile and [Benzo-15-crown-5]-(4,5-bis-methylthio)maleonitrile have been prepared by the reaction of different alkyl halides such as 1,2-bis(brommethyl)benzene and 4,5-bis-(brommethyl)[benzo-15-crown-5] with dithiomaleonitrile disodium salt.
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Conclusion & Impact:Both compounds are characterized by IR, Mass, NMR spectroscopy as well as elemental analysis.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Macrocycle · maleonitrile · crown ethers

Abstract

In this study, the synthesis and thermal properties of two novel maleonitriles bearing 8-membered heterocyclic derivatives is described first time. New maleonitriles, benzo-(1,2-bis-methylthio)maleonitrile and [Benzo-15-crown-5]-(4,5-bis-methylthio)maleonitrile have been prepared by the reaction of different alkyl halides such as 1,2-bis(brommethyl)benzene and 4,5-bis-(brommethyl)[benzo-15-crown-5] with dithiomaleonitrile disodium salt. Both compounds are characterized by IR, Mass, NMR spectroscopy as well as elemental analysis.

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Cite This Article

ERDOĞMUŞ, A. (2016). SYNTHESIS AND THERMAL PROPERTIES OF NOVEL MALEONITRILES. Sigma Mühendislik ve Fen Bilimleri Dergisi, Cilt: 34 - Sayı: 2, 153–158. https://ajindex.com/articles/419271

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