Various parameters such as Schiff base, supporting electrolyte concentrations, accumulation potential and deposition time were optimized.
📌 3 Key Takeaways
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Objective & Hypothesis:In this work, a new method for the determination of germanium in the presence N-(4-hydroxyphenyl)-3,4-dihydroxybenzaldimine was developed by using adsorptive stripping voltammetry.
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Key Findings & Data:In this work, a new method for the determination of germanium in the presence N-(4-hydroxyphenyl)-3,4-dihydroxybenzaldimine was developed by using adsorptive stripping voltammetry.
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Conclusion & Impact:Various parameters such as Schiff base, supporting electrolyte concentrations, accumulation potential and deposition time were optimized.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters
Abstract
In this work, a new method for the determination of germanium in the presence N-(4-hydroxyphenyl)-3,4-dihydroxybenzaldimine was developed by using adsorptive stripping voltammetry. Various parameters such as Schiff base, supporting electrolyte concentrations, accumulation potential and deposition time were optimized.
Özet
Bu çalışmada, N-(4-hidroksifenil)-3,4-dihidroksibenzaldimin varlığında kare dalga adsorptif sıyırma voltametrisi ile eser miktarda germanyum tayini için yeni bir yöntem geliştirilmiştir. Ligand ve destek elektrolit konsantrasyonları, biriktirme potansiyeli ve biriktirme süresi gibi çeşitli parametreler optimize edilmiştir.
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Cite This Article
YÜKSEL, M. (2003). Determination of germanium in the presence of Schiff base by adsorptive stripping voltammetry. Technology, Cilt: 6 - Sayı: 1, 17–24. https://ajindex.com/articles/359671
Nazerenko, V.A. 1974. Analytical Chemistry of Germanium, J. Wiley, New York
Shi, J.,and Jiao, K., 1995. Adsorptive Complex Catalytic Polarographic Determination of Germanium in Soils and Vegetables. Anal.Chim. Acta, 309; 103-109
Nashine, N., and Mishra, R.K., 1994. Selective Extractive Spectrophotometric Determination of Germanium with N-hydroxy-N,N’-diphenylbenzamidine and Iodide. Anal. Chim. Acta, 285; 365-368
Abbasi, S.A. 1988. Atomic Absoption Spectrometric and Spectrophotometric Trace Analysis of Germanium in Enviromental Samples with N-p-Bromophenyl-2-Furylacrylohydroxamic Acid and phenylfluorone. Intern. J.Environ. Anal. Chem., 33(2), 149-160. 24 Adsorptif Siyirma Voltametrisi İle Schiff Bazi Varliğinda Germanyum Tayini 5. Scleich, C., and Henze, G. 1990. Some New Aspects for The Determination by Extraction-Specdtrophotometry and Atomic Absorption Spectrometry. Fresenius’ J.Anal. Chem. 338, 140-44
Sohrin,.Y,1991.Determination of Organometallic and Inorganic Germanium by Inductively Coupled Plasma Atomic Emission Spectrometry. Anal.Chim. Acta, 247;1-6
Thompson, M., and Phalavanpour, B., 1979. Reduction of Tin and Germanium To Hydrides for Determination by Inductively-Coupled Plasma Atomic Emission Spectrometry. Anal.Chim. Acta, 109; 251-58
Khan, A.S. and Chow, A., 1990. X-ray Fluorescence Spectrometric Determination of Germanium after Extraction with Polyurethane foam. Anal. Chim. Acta., 238; 423-426
Hasebe, K.,Hikima, S., Kakizaki, T., and Yoshida, H. 1989. Analytical Science, 5, 225
Hasebe, K., Hikima, S., Kakizaki, T. Iwashimizu, T., and Aoki, K. 1990. Trace Determination of Germanium by Means of Adsorption Waves in Differential-Pulse Polarography. Analyst, 115; 413-416
McCrory-Joy, C., Rosamilia, J.M. 1982. Differential Pulse Polarography of Germanium(IV), Tin(IV), Arsenic(V), Antimony(V), Selenium(IV) and Tellurium(VI) at The Static Mercury Drop Electrode in Catechol-Percholorate Media. Anal. Chim. Acta, 142; 231-238
Aguilar, J.C., and Gyves, J. 1995. Determination of germanium(IV) in sulphide ores by differantial pulse polarography in pyrogallol-sulfuric acid media. Anal.Chim. Acta, 306, 243
Karpinski, Z.J., Polosak, A., and Kublik, Z. 1980. Anodic Stripping Voltammetry of Germanium at The Hanging Mercury Drop Electrode. Anal. Chim. Acta, 120; 55-64
Dexiong, F., Peıhıuı, Y., and Zhaolıang, Y., 1991. Determination of Germanium by Potentiometric Stripping Analysis. Talanta, 38(12); 1493-1498