The microanalysis and spectral data of the synthesized compounds are in full agreement with their molecular structure.
📌 3 Key Takeaways
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Objective & Hypothesis:The reaction of amidrazones 1 with a-haloesters 2 formed 1,3,5-substituted 4,5-dihydro-1,2,4-triazin-6-ones (4a-z) rather than 1,2,4-triazin-5-one derivatives (5a-z).
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Key Findings & Data:The reaction of amidrazones 1 with a-haloesters 2 formed 1,3,5-substituted 4,5-dihydro-1,2,4-triazin-6-ones (4a-z) rather than 1,2,4-triazin-5-one derivatives (5a-z).
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Conclusion & Impact:The microanalysis and spectral data of the synthesized compounds are in full agreement with their molecular structure.
The reaction of amidrazones 1 with a-haloesters 2 formed 1,3,5-substituted 4,5-dihydro-1,2,4-triazin-6-ones (4a-z) rather than 1,2,4-triazin-5-one derivatives (5a-z). The microanalysis and spectral data of the synthesized compounds are in full agreement with their molecular structure.
Özet
The reaction of amidrazones 1 with a-haloesters 2 formed 1,3,5-substituted 4,5-dihydro-1,2,4-triazin-6-ones (4a-z) rather than 1,2,4-triazin-5-one derivatives (5a-z). The microanalysis and spectral data of the synthesized compounds are in full agreement with their molecular structure.
DALLOUL, H. M., BOYLE, P. H. (2007). Synthesis of Nitrogen-Containing Heterocycles from the Reaction of Amidrazones with a-Haloesters. Turkish Journal of Chemistry, Cilt: 31 - Sayı: 2, 141–147. https://ajindex.com/articles/185029
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