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Journals / Bilecik Şeyh Edebali Üniversitesi Fen Bilimleri Dergisi / 2019 / Cilt: 6 Sayı: 2

Synthesis and characterization of Cu-doped NaPO3 glasses

Cu katkılı NaPO3 camlarının sentez ve karakterizasyonu

Serhat Keser(FIRAT UNIVERSITY)0000-0002-9678-1053
Tankut Ateş(FIRAT UNIVERSITY)0000-0002-4519-2953
Ömer Kayğılı(FIRAT UNIVERSITY)0000-0002-2321-1455
Pages
552–561
Publication Date
2019-12-26
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

It was determined that the morphology of the as-produced sodium phosphate glasses was affected by Cu-doping .

📌 3 Key Takeaways

🎯
Objective & Hypothesis:The presented work has been aimed to investigate the effects of Cu-doping on the structural and morphologic properties of NaPO 3 (sodium metaphosphate or sodium phosphate) glasses.
📊
Key Findings & Data:Cu-containing NaPO 3 glasses at different ratios were synthesized at 700 °C.
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Conclusion & Impact:It was determined that the morphology of the as-produced sodium phosphate glasses was affected by Cu-doping .
🔬Design:Araştırma Makalesi
📍Scope:Comprehensive Sample
⚙️Variables:X-ışını kırınımı (XRD) · FT-IR · Morfoloji

Abstract

The presented work has been aimed to investigate the effects of Cu-doping on the structural and morphologic properties of NaPO 3 (sodium metaphosphate or sodium phosphate) glasses. Cu-containing NaPO 3 glasses at different ratios were synthesized at 700 °C. The characterization process of the as-synthesized glasses was performed using Fourier transform infrared (FTIR), X-ray diffraction (XRD) and scanning electron microscopy (SEM). It was determined that the single phase of the as-produced samples was the NaPO 3 with the orthorhombic crystal structure. Furthermore, it was observed that the Cu-addition caused significant variations in the amount of crystallinity, crystallite size and lattice parameters of the as-produced sodium phosphate glasses. It was determined that the morphology of the as-produced sodium phosphate glasses was affected by Cu-doping .

Özet

Sunulan çalışma, NaPO 3 (sodyum metafosfat ya da sodyum fosfat) camlarının yapısal ve morfolojik özellikleri üzerinde, Cu katkısının etkilerinin incelenmesini amaçlamaktadır. Farklı oranlarda Cu katkısı içeren NaPO 3 camları 700 °C’de sentezlendi. Sentezlenen camların karakterizasyon işlemi Fourier dönüşümlü kızılötesi (FTIR), X-ışını kırınımı (XRD) ve taramalı elektron mikroskopisi (SEM) ile gerçekleştirildi. Üretilen numunelerin sahip oldukları tek fazın ortorombik kristal yapıdaki NaPO 3 olduğu belirlendi. Ayrıca, Cu katkısının üretilen sodyum fosfat camlarının kristalleşme miktarı, kristal büyüklüğü ve örgü parametrelerinde önemli değişimlere sebep olduğu gözlendi. Üretilen sodyum fosfat camlarının morfolojisinin Cu katkılanmasıyla etkilendiği belirlendi.

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Cite This Article

Keser, S., Ateş, T., Kayğılı, Ö., *, S. K. (2019). Synthesis and characterization of Cu-doped NaPO3 glasses. Bilecik Şeyh Edebali Üniversitesi Fen Bilimleri Dergisi, Cilt: 6 Sayı: 2, 552–561. https://doi.org/10.35193/bseufbd.596180

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