Journals / Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering / 2024 / Volume: 66 Issue: 2

Synthesis and characterization of graphene oxide using modified hummers method

Pages
19–35
Publication Date
2024-12-31
DOI
—
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

FT-IR, RAMAN, XRD, SEM, and EDS analyses were performed for characterization, yielding results consistent with findings reported in the literature.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:Since graphene is expensive and relatively difficult to produce, significant efforts have been made to develop effective and inexpensive methods for creating and utilizing graphene [1], derivatives, or related materials.
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Key Findings & Data:GO is typically synthesized as a powder, in dispersion, or substrate coating.
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Conclusion & Impact:FT-IR, RAMAN, XRD, SEM, and EDS analyses were performed for characterization, yielding results consistent with findings reported in the literature.
🔬Design:Text.Serial.Journal
📍Scope:Comprehensive Sample
⚙️Variables:Graphene oxide · graphite powder · modified hummer’s method

Abstract

Since graphene is expensive and relatively difficult to produce, significant efforts have been made to develop effective and inexpensive methods for creating and utilizing graphene [1], derivatives, or related materials. Graphene oxide (GO) is one such material. It consists of a single layer of atoms produced through the strong oxidation of cheap and abundant graphite. GO is an oxidized form of graphene containing oxygen-functional groups. Due to its ability to disperse in water and other solvents, GO is easy to process and can even serve as a precursor for graphene production. Although GO is not a good conductor, various processes can enhance its properties. GO is typically synthesized as a powder, in dispersion, or substrate coating. There are four primary methods for synthesizing GO: Staudenmaier, Hofmann, Brodie, and Hummers, with many variations available and ongoing improvements aimed at achieving better results and more cost-effective processes. The efficiency of the oxidation process is typically evaluated by the carbon-to-oxygen ratio of GO. In this study, graphene oxide was synthesized from graphite using a modified Hummers method. In this modification, an ice bath and sodium nitrate (NaNO3) were omitted, and the synthesis was conducted at room temperature. FT-IR, RAMAN, XRD, SEM, and EDS analyses were performed for characterization, yielding results consistent with findings reported in the literature.

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Cite This Article

Ahanibarough, M., Özkorucuklu, S. P. (2024). Synthesis and characterization of graphene oxide using modified hummers method. Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering, Volume: 66 Issue: 2, 19–35. https://ajindex.com/articles/1023447

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